Moving from TRACE GC Ultra to………..Moving from TRACE GC Ultra to ...... • How Thermo TRACE GC Ultra was structurally concepted: • Mainframe - Oven Overview • Injectors - Detectors Overview • Detector base body concept Gas ModulesOverview Detectors Overview 2 Mainframe & Oven Overview DGFC module Detectors DPFC module Injectors detectors cassette Electronics Detectors base bodies Keypad 3 Injections Overview True cold On-Column Split/Splitless PTV Packed and wide-bore columns 4 Detector base body concept It allows simple detector interchangeability GC top deck It ensures flexibility without adding complexity Detector Base body Oven 6 Detector base body concept A common base which provides the detector with main heating and gas feeding All detectors are available with both Digital Gas Flow Control (DGFC) and conventional pressure regulators (nonDGFC) 7 . ..................... ................Moving from TRACE GC Ultra to...... 8 ....... TRACE 1300 Series Modular Concept 9 .......... 2 versions: 220V and 120V • Injector modules include injector body. . 10 .1310 Series Modular Concept • A main electronic module that includes: main CPU.. • Detector modules include detector cell and electronics for signal amplifier –digitalization..TRACE 1300 . power supply.. • TRACE 1300 – TRACE 1310 can accommodate 2 inlet and 2 detector modules (2 channels) self-recognized • Additional external devices can be located into dedicated housing.. oven control. electronics for injector temperature and carrier gas control. for temperature and detector gas control.. upgrading. or change of configuration • Possibly modules would be replaced without requiring a field service engineer 11 .TRACE 1300 .1310 Series Modularity Advantages • Modules can be tested (also analytically) separately prior testing the assembled unit • Modules can be shipped separately and assembled during the installation in field • Modules can be kept in stock for fast replacement. Trace GC 1310: Touch screen interface provides instant access for ease of use and local control 12 .1310 Modular Concept Trace GC 1300: Local built-in ultrasimplified user interface .two buttons and four LEDs.TRACE 1300 . TRACE 1300 .1310 Series Modular Concept Where the parts were on TRACE GC Ultra and Where they are now on TRACE 1300 Series 13 . 1310 • Injector Module • DPFC/DCC module • EPC Board • Thermoregulator (I/O Feedback board) • Power control 14 .TRACE GC Ultra • Injector TRACE 1300 . TRACE GC Ultra • • • • • Detector Base body DGFC module Detector board Thermoregulator (I/O Feedback board) TRACE 1300 – 1310 • Detector Module • EPC board • Power control 15 . TRACE GC Ultra • • • • CPU Board I/O Feedback board Mother board Power supply TRACE 1300 – 1310 • Electronic Compartment 16 . TRACE GC Ultra • GC Keypad TRACE 1300 – 1310 • User Interfaces 1300 • User Interfaces 1310 17 . TRACE 1310 Instrument Control 18 . TRACE 1310 Configuration 19 . TRACE 1310 Diagnostics 20 . TRACE 1310 Status 21 . TRACE 1310 Maintenance *When Graph Pack adapters will be used. the column insertion into the Injector and Detector inlets must be added of 12mm. 22 . 1310 HW connectivity • GC Control through Ethernet IP address • Direct connection to PC (reversed RED cable) • Connection to LAN (standard GREY cable) • • Two RS-232 ports for Autosampler control Thermo Fisher bus I2C with 5V power for additional auxiliary devices 23 .TRACE 1300 . 1310 Ethernet configuration • • • MAC address fixed and assigned in the factory IP Address -> need to be assigned TCP Port -> 2551 (different from the one used on Trace GC) • • Chrom-Card and Xcalibur accepts TCP Port=2551 ChromQuest has a different TCP Port -> need to be changed in TRACE 1300-1310 • Ethernet Configuration details listed within “Diagnostic” menu 24 .TRACE 1300 . TRACE 1300 – 1310 Set up • • From the PC. launch the Setup. press OK. Do not change any file inside. 25 . This SW load the whole package zip file as it is.exe file named TR1300ST (Service Tool) entering ThermoFisher as password. then. 26 .TRACE 1300 – 1310 Set up • Automatically the SCAN will start to check how many systems are present. automatically the two dedicated options will be activated 27 .TRACE 1300 – 1310 Set up • Selecting the instrument on which IP set-up and Firmware updating must be performed. TRACE 1300 – 1310 IP Set up • Selecting IP Set-up a new page will be shown where GC name and IP address can be modified. 28 . TRACE 1300 – 1310 F/W update Selecting F/W update a new page will be shown. 29 . or. ) Do not change any file inside.... click on “Browse package name” and select where the package with the new firmware version is present (C: or USB.. TRACE 1300 – 1310 F/W update • On the new page will be shown the TRACE 1300-1310 configuration with the current F/W version of the modules installed and the package of the new firmware version. 30 . Select Update to start the F/W updating. .. 31 ...TRACE 1300 – 1310 F/W update • F/W updating in progress.......... • Click Done to close the program.TRACE 1300 – 1310 F/W update • At the end of the F/W updating. 32 . all the status cell must be OK. 1310 HMI SW update from USB stick • HMI SW can be updated through the USB port positioned below the touch screen 33 .TRACE 1300 . TRACE 1300 .1310 HMI SW update from USB stick Configuration 34 . .....TRACE 1300 – 1310 Series ..more in depth 35 ........ Split & Purge) • 2 Removable Filters (Carrier & Split) 36 .TRACE 1300 – 1310 SSL Injector Module • • • • Manifold (Plumbing) Removable SSL Injector Body 2 Electronic Boards 3 Solenoid Valves (Carrier. TRACE 1300 – 1310 SSL Injector Module 0 10 20 30 • Designed to have a cool head and septum. Depth (mm) 40 50 60 70 80 90 100 100 • Septa is kept below 150°C even with inlet set to 350°C • Lower septum bleeding (siloxanes) • No septum sticking • Lower air (oxygen) diffusion • Longer septa lifetime • The cool head SSL is optimized for cold needle injection 150 200 250 T (°C) 300 350 400 37 . 1 KPa along the entire scale • Flow ranges: • • • • • • • • • Column flow from 0.1 to 100 ml/min. • Pneumatics: Electronic control only Constant pressure Constant flow Flow regulation through calculated pressure Pressure or flow programming in three ramps and four plateaus • • • • • • Pressure range: • 0 to 1000 KPa. with a resolution of . and stability of 0.015 KPa. • Operating modes: 38 .c. with resolution of 0.TRACE 1300 –1310 SSL Technical Specification • Temperature range: • Maximum temperature 400º C with temperature settings resolution of 1º C units • Temperature stability 1º C • Heater cartridge 80W 48Va.01 ml/min Split flow from 10 to 1250 ml/min He with resolution of 1mL/min Septum purge flow from 0 to 50 ml/min with resolution of 1mL/min Ambient temperature and pressure compensation Gas saver function Split /Split less Surged Split/Surged Split less Large Volume Split less Back-flush capability (*) NOTE: Standard SSL CANNOT BE converted to SSL BKF a new module MUST BE requested. TRACE 1300 – 1310 PTV Injector Module • Manifold (Plumbing) • Removable PTV top head • Removal of bottom column connection for easier cleaning of internal body • 2 Electronic Boards • 3 Solenoid Valves (Carrier. Split & Purge) • 2 Removable Filters (Carrier & Split) • Cooling Fan 39 . TRACE 1300 – 1310 PTV Injector Module • Removal top body plus tubing for easier cleaning • Removal of bottom column connection for easier cleaning of internal body 40 . 1 KPa along the entire scale Flow programming: 0.TRACE 1300 – 1310 PTV Technical Specification • Temperature operating range: • • • • • • • • • • • • • • • • • • Maximum temperature 450º C with temperature settings resolution in 1º C units Temperature stability 1º C maximum at 250º C for 30 minutes Temperature program rate up to 14.1 to 100 ml/min.c. Splitless. Solvent Split (Large Volume) • Back-flush capability (*) NOTE: Standard PTV CANNOT BE converted to PTV BKF a new module MUST BE requested. Capable of sub ambient operation to -50º C with LN2.015 KPa. Three different temperature programmable ramps. and stability of 0.01 ml/min Independent pressure/flow set points during injection Ambient pressure compensation. 41 . four plateaus Electronic control only Constant pressure Constant flow (Flow regulation through calculated pressure) Pressure or flow programming in three ramps and four plateaus Pressure programming: 0 to 1000 KPa.5ºC/sec Heater assy 120W 48Va. with a resolution of . 0º C with CO2 Sub-ambient control will be optional and should not add cost to base unit. Control of split flow in 1mL/min from 10 to 1250 mL/min He Gas consumption saver Purge flow from 0 to 50 ml/min • Pneumatics: • Operating modes: • Split. with resolution of 0. TRACE 1300 – 1310 Injector Modules SSL Body PTV Head 42 . TRACE 1300 – 1310 FID Detector Module • • • • Manifold (Plumbing) Detector body 2 Electronic Boards 3 Solenoide Valves (Air. Hydrogen & Make up) 43 . 450º C • Flameout detection and warning • Automatic flame re-ignition with shutdown of gases upon failure (3 times) • MDA: <2 pg carbon/sec as propane • Linear dynamic range 10^7 • Acquisition rate up to 300 Hz 44 .TRACE 1300 – 1310 Detector Specifications • FID Technical Specifications • Maximum operating temperature. TRACE 1300 – 1310 Detector Specifications • TCD Technical Specifications • • • • • • Maximum operating temperature. filament ambient to 450º C Operating modes: constant mean temperature Filament protection in case of carrier gas failure Compatible with Fe/Ni or W/Re filaments MDA: 600 pg ethane/ml He carrier Linear dynamic range >= 10^6 45 . 400º C. 05 pg N/s or better.TRACE 1300 – 1310 Detector Specifications • NPD Technical Specifications • Compatibility with DET’s TID-2. • Heating Current setting: 1.000 to 1 gP/gC or better. • MDL: Nitrogen: 0. • Maximum Operating Temperature: Up to 450°C.000 to 1 gN/gC or better. • Dynamic and Linear Range: Dynamic range of response: 10E6.00 to 3. P/C = 200.50 A (or different range according to the source requirements) in 0. Agilent’s BLOS and other DET TID types. Linear range: 10E4 or better. • Source protection in case of gas failure 46 . • Selectivity: N/C = 50.02 pg P/s or better.01 steps. Phosphorus: 0. • Data acquisition rate: Up to 300Hz to be compatible with fast and ultrafast GC. pulse modulated MDA <= 5 fg Lindane Linear dynamic range: >10^4 Ar/CH4 make-up Equipped with removable collector electrode for local maintenance 47 .TRACE 1300 – 1310 Detector Specifications • ECD Technical Specifications • • • • • • • Maximum operating temperature: 400º C Cell volume <= 150 µl Acquisition rate up to 100 Hz Operating mode: constant current. TRACE 1300 – 1310 Pneumatic Net 48 . TRACE 1300 – 1310 Gas Net Assembly 49 . TRACE 1300 – 1310 Gas Net Location 50 . TRACE 1300 – 1310 Components location Hermes back view electronic box detector module injector module gases inlet main switch toroidal transform fan motor oven Hot air outlet duct door insulation material H2 sensor (optional) 51 . heating element RTD front view back view 52 . • The serial or parallel heaters wiring is driven by the electronic box. according to the tension rate.TRACE 1300 – 1310 Oven heating • The tension rate changes from 230V to 120V but not the baffle. 1 x 500VA sec. 1 x heater 1 x fan (oven) 53 .TRACE 1300 – 1310 Module “Electronics” Backplane CONTROL AREA Connections for: 2 x injector 2 x detectors 1 x PT100 1 x door switch 1 x stepper (flaps) 1 x H2 sensor 3 x 24V auxiliary POWER AREA Connections for: 1 x main line 1 x 500VA pri. TRACE 1300 – 1310 Module “Electronics” Electronic compartment Fan Handles Breaker Oven & Power Power switching External Interface Main CPU 54 . TRACE 1300 – 1310 Series Autosamplers Injection position 55 Inlet maintenance position . TRACE 1300 – 1310 Series Autosamplers Injection position Inlet Maintenance position 56 . TRACE 1300 – 1310 Series Autosamplers 57 . TRACE 1300 – 1310 Series Autosamplers 58 . TRACE 1300 .1310 Series & ISQ TRACE 1310 & ISQ must look like a single instrument when coupled 59 . TRACE 1300 – 1310 Series Questions? 60 .