Thermal Analysis Product Literature / Technical PapersTA Instruments, 109 Lukens Drive, New Castle DE 19720, USA Now available for download from the TA Instruments website www.tainst.com Or complete and return this form (either fax, mail or give to your TA Instruments Representative) and the requested information will be sent by mail. NAME_________________________________ TITLE _________________________ AFFILIATION __________________________________________________________ ADDRESS ______________________________________________________________ CITY __________________________ STATE _____ POSTAL CODE ____________ TELEPHONE __________________________ FAX ___________________________ E-MAIL ________________________________________________________________ □__Please have a representative call to discuss my potential applications. Order the Applications Library on CD-ROM! A complete collection of Applications Literature is available for purchase on CD-ROM, p/n 925700.901. 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The Applications Library CD provides the information you need at your fingertips when you need it. 1 TA 001k Measuring Expansion and Contraction Simultaneously Making Accurate DSC and MDSC Specific Heat Capacity Measurements with the Q1000 Tzero DSC Measuring the Glass Transition of Amorphous Engineering Thermoplastics Using the DMA Q800 for ASTM International D 648 Deflection Temperature Under Load Dynamic Mechanical Analysis and its Advantages for Deflection Temperature Under Load Measurements Weight Loss Determined from Mass Spectrometry Trend Data in a Thermogravimetric/Mass Spectrometer System Use of the Photocalorimeter Accessory (PCA) with Tzero DSC Use of Tzero and Modulated DSC for Characterization of Milk Products 2 TA 001k .Theory & Applications Modulated Thermogravimetric Analysis: A New Approach for Obtaining Kinetic Parameters Thermal Analysis Review: Modulated DSC® Theory Thermal Analysis Review: Modulated DSC Compendium Basic Theory and Experimental Considerations.THERMAL ANALYSIS _____________________________________________________________ PRODUCT LITERATURE □ □ □ □ □ □ □ □ □ □ □ TA256 TA202 TA023 TA237 □ □ TA211 TA210 □ □ SP00010 RN017 TA264 TA263 TA284 TA028 Brochure: Thermal Analysis Systems Product Overview Brochure: Rheology Systems Product Overview Brochure: Q Series™ DSC Brochure: Q Series™ TGA & SDT Brochure: Q Series™ DMA Brochure: Q Series TMA Brochure: Pfeiffer ThermoStar Mass Spectrometer Brochure: Thermal Advantage Software Product Bulletin: Certified Calibration Standards Thermal Analysis Review: High Resolution TGA. Parts and Accessories Catalogue Rheology Literature List THERMAL ANALYSIS APPLICATIONS BRIEFS □ □ TA319 TA318 □ □ TA317 TA316 □ TA315 □ TA314 □ TA313 □ TA312 □ TA311 □ TA310 □ □ TA309 TA308 □ TA307 □ TA306 □ □ TA305 TA304 Heat Content of Coal by Pressure DSC Thermogravimetry: A Great Tool for Flue Gas Desulfurixation Solids Analysis Methodology for Thermal Analysis of Excipients Validation of Thermogravimetric Analysis Performance Using Mass Loss Reference Materials Characterization of Polymorphic Transitions in a Pharmaceutical by DSC and MDSC Quantification of Polybutadiene in an Elastomeric Blend by Tzero DSC and Modulated DSC Interlaboratory Kinetics Studies Using ASTM International Standards E2041 and E698 and Trityl Azide Thermal Conductivity Measurements of Conductive Epoxy Adhesives by MDSC Modulated Thermomechanical Analysis . Part V: Reducing Thermal Lag How Tzero™ Technology Improves DSC Performance.□ TA303 □ TA302 □ TA301 □ TA300 □ □ □ □ □ TA299 TA297 TA296 TA295 TA294 □ □ □ TA293 TA292 TA291 □ □ □ □ □ TA290 TA289 TA287 TA286 TA285 □ TA283 □ TA282 □ □ TA281 TA280 □ TA279 □ TA278 □ □ □ □ □ □ TA277 TA276 TA275 TA274 TA273 TA272 □ TA269 □ TA268 □ □ □ TA267 TA266 TA265 □ □ □ □ □ □ TA262 TA258 TA257 TA253 TA250 TA248 Quantitative Determination of Amorphous and Crystalline Drug in Polymer Microspheres DSC Detection of Polymorphism in Pharmaceutical Anhydrous Dexamethasone Acetate Improvements in DMA Measurements Using Low-Fiction 3-Point Bending Clamps DSC Step Annealing for Fingerprinting Molecular Structure in Poly(vinylidene fluoride) Physical Aging and Fragility of Amorphous Polyethylene Terephthalate High Heating Rate DSC Physical Aging and Fragility of Amorphous Sucrose by DSC Purity Determination and DSC Tzero Technology Recertification of the Polyethylene Oxidation Induction Time Reference Material α-Monohydrate Phase in Lactose by DSC Isothermal Crystallization of Polypropylene by DSC Use of Multiple Heating Rate DSC and Modulated Temperature DSC to Detect and Analyze Temperature-Time-Dependent Transitions in Materials Determining Percent Solid in an Edible Fat Evaluation of Fiber Heatsetting by MDSC Time-Temperature Superposition Using DMA Creep Data Determining Percent Solid in a Polymer Blend How Tzero™ Technology Improves DSC Performance. Part III: The Measurement of Specific Heat Capacity How Tzero™ Technology Improves DSC Performance. Part IV: MDSC Enhancement Tzero™ DSC and Peak Shape of First Order Transitions Isothermal Crystallization Using the Q Series™ DSC and Liquid Nitrogen Cooling System How Tzero™ Technology Improves DSC Performance. Part II: Peak Shape and Resolution Characteristics of Tg Detection Using Micro Thermomechanical Analysis Determination of Polymer Crystal Molecular Weight Distribution by DSC Impact of Tzero™ Technology on the Measurement of Weak Transitions Impact of Tzero™ Technology on DSC Resolution Design of a New DSC Cell with Tzero™ Technology How Tzero™ Technology Improves DSC Performance. Part VI: Simplifying Temperature Calibration for Cooling Experiments How Tzero™ Technology Improves DSC Performance. Part I: Flat Baseline and Glass Transition Measurements DSC Resolution and Dynamic Response Improvements Obtained by a New Heat Flow Measurement Technique DSC Baseline Improvements obtained by a New Heat Flow Measurement Technique High Heating Rate Modulated DSC Using Tzero™ DSC Technology Practical Benefits of Using Heat Capacity Versus Heat Flow Signals Precision and Bias of the ASTM Test E1952 for Thermal Conductivity by Modulated DSC Time-Temperature Superposition Tutorial for Advantage Software Characterization of Surface Morphology Changes by Micro-Thermal Analysis Micro-Thermal Analysis .An Holistic Approach to Materials Characterization Kinetic Parameters of Overlapping Coal Decomposition Reactions by MTGA™ Determining Volatile Organic Carbon by Differential Scanning Calorimetry Recent Developments in the Application of Thermal Analysis to Polyolefins 3 TA 001k . R. R. L. Blaine and B. C. M. T. Mary B. Hahn. L. Blaine. L. R. Harris “A Proposed Reference Material for Oxidative Induction Time by Differential Scanning Calorimetry”. JOURNAL OF THERMAL ANALYSIS “A Faster Approach to obtaining Kinetic Parameters”. Groh “Turning Up the Heat”.A Review of DSC Experimental Effects”. L. Blaine. AMERICAN LABORATORY “Dynamic Mechanical Analysis of Polymers”. AMERICAN LABORATORY “Oxidative Induction Time . Lundgren. K. J. Blaine. Harris 4 TA 001k . J. R.□ □ □ □ TA246 TA238 TA231 TA227 □ TA226 □ TA222 □ □ TA144 TA143 □ TA141 □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ TA138 TA137 TA136 TA135 TA134 TA133 TA132 TA131 TA130 TA129 TA128 TA127 TA126 TA125 TA123 TA122 TA121 TA120 TA119 TA108 TA073 TA039 RH088 RH087 RH086 Time-Temperature Superposition Evaluation of Hazards Potential by DSC TGA Evaluation of Zeolite Catalysts Characterization of Melting Phenomena in Linear Low Density Polyethylene by Modulated DSC® Characterization of a Polycarbonate/Polyetherester Blend Using Modulated DSC Isothermal Crystallization Made Easy: A Simple Model and Modest Cooling Rates Application of Time-Temperature Superposition Principles to DMA A Comparison of Commercially Available DSC Kinetic Methods for Evaluating Bismaleimide Resins High Resolution TGA/Mass Spectroscopy Characterization of Fuel Oil Transport Additives The Correlation of TMA with ASTM Modulus Data Detection of the Glass Transition in Metal Glasses by DSC and DMA Evaluation of Metal Catalysts Use of TGA to Distinguish Flame-Retarded Polymers from Standard Polymers Kinetics of Drying by TGA Measurement of Moisture Effects on the Mechanical Properties of 66 Nylon Oxidative Stability of Oils and Greases Detection of Beta Transus in Titanium Alloys by DTA Polypropylene Impact Resistance by DMA Proximate Analysis of Coal and Coke Polyester Heat History Detection by DSC Differentiation Between Grades of ABS by Hi-Res™ TGA Gelation of Epoxy-Glass Prepreg by Parallel Plate Rheometry Estimation of Polymer Lifetime by TGA Decomposition Kinetics Determination of Polymer Crystallinity by DSC Determination of Carbon Black Pigment in Nylon 66 by TGA Oxidative Stability of Polyethylene Terephthalate Transition Temperature of Liquid Samples by TMA Dynamic Mechanical Analysis of Food Products Determination of Layer Thickness in Multilayer Packaging Films A Review of DSC Kinetic Methods Interpreting Unexpected Events and Transitions in DSC Results Characterization of Cured Rubber by DMA Detection of an Adhesive Layer Between Polyester Films Using DMA Guideline for Using Time-Temperature Superpositioning THERMAL ANALYSIS TECHNICAL PUBLICATIONS □ TA271 □ □ TA270 TA251 □ TA245 □ TA236 □ TA235 □ TA233 “Improved DSC Performance Using Tzero™ Technology” R. Kelly. B. J. Danley. Foreman. THE SUPPLY LINE “Obtaining Kinetic Parameters by Modulated Thermogravimetry”. Kunze. J. AMERICAN LABORATORY. Hassel. Marcozzi “The Case for a Generic Definition of Differential Scanning Calorimetry”. A. Gill “Modulated Differential Scanning Calorimetry”. Foreman. W. Thomas. C. Sauerbrunn. “Calorimetric and Rheology Investigation of Modified Polypropylenes”. Lever. J. L. Hawkins. Lundgren. Foreman and K. A. Sauerbrunn. R. January 2004 _____________________________________________________________________ THERMAL ANALYSIS APPLICATIONS NOTES □ □ □ □ □ TN057 TN056 TN055 TN054 TN053 Exceptions to the A2LA Traceability Policy Humidity Fixed Points Regulatory Position Certificate of Conformance ISO 17025. P. J. H. P. S. G. Foreman. A. Dallas. C. Van Mele. R. Seyler “Measurement of the Physical Properties of Engineering Thermoplastics Using Thermal Analysis”. Gill. R. Foreman. L. Marcus. J. C. Groves. R. D. A. Wolkowics “Differential Scanning Calorimetry for Boiling Points and Vapor Pressure”. S. J. T. Franck.L. K. Crowe. A. L. K. B. A. D. Armbruster. S. S. S.□ TA230 □ TA229 □ TA228 □ TA220 □ TA219 □ TA218 □ TA208 □ TA201 □ TA090 □ TA086 □ □ TA085 TA083 □ TA082 □ TA081 □ □ TA075 TA072 □ TA070 □ TA052 □ TA038 □ TA037 □ □ TA036 RH089 “ Heat Capacity Measurements Using Quasi-Isothermal MDSC®”. S. Sauerbrunn. PI QUALITY “The Combined Use of Thermal Analysis and Rheology in Monitoring and Characterizing Changing Processes in Materials”. Sircar “Exploring the Sensitivity of Thermal Analysis Techniques to the Glass Transition”. Reading “Dynamic Mechanical Analysis . M. INTERNATIONAL LABMATE “Development of a New Oxidation Stability Test Method for Greases Using a Pressure Differential Scanning Calorimeter” In-Sik Rhee. Foreman. A2LA and QS9000 ISO Certificate 5 TA 001k . R. Smith. Cationic and Hybrid Photopolymers”. Klinger. G. Sauerbrunn. R. M.A Versatile Technique for the Viscoelastic Characterization of Materials”. B. L. L. ASTM MANUAL 17 “Modulated DSC® Evaluation of Isothermal Cure and Vitrification for Thermoset Systems”. Blaine “Coatings Characterization by Thermal Analysis”. N. NLGI SPOKESMAN “Tensile Modulus of Plastic Films”. S. S. J. S. R. S. F. Gill “Thermal Conductivity of Polymers. J. A. Sauerbrunn “Differential Photocalorimetry: Advancements for the Analysis and Characterization of Free Radical. Foreman. A. A. Neag. P. Blaine “Decomposition Kinetics Using TGA”. Aubuchon “Dynamic Mechanical Analyzers: How Do They Work?” J. Glasses and Ceramics by Modulated DSC” “High Pressure Oxidative Induction Time Analysis by DSC” “Analysis of Elastomer Vulcanizate Composition by TG-DTG Techniques”. Jones. Shickel “Using Temperature to Control Quality”. M. M. Van Assche. C. R. Blaine “The Property-Performance Differences Between Two Blended Polypropylene Fibers”. J. K. R. Reed “Estimation of Bias in the Oxidation Induction Time Measurement by Pressure DSC”. R. I. Rahier. R. S. A. A. Van Hemelrijck. P. R. C. ASTM D1600 Sapphire Specific Heat Capacity Literature Values Enhances DSC Glass Transition Measurements Boiling Point and Vapor Pressure Measurements by Pressure DSC Hints for Good Purity Determinations DSC Cell Cleaning THERMAL ANALYSIS SOLUTIONS □ TS084 □ TS083 □ □ TS082 TS081 □ □ □ TS080 TS079 TS075 □ □ □ TS073 TS072 TS071 □ □ TS070 TS069 Using High-Volume Sample Pans to Characterize the Curing Reaction of a Phenolic Resin Sample Glass Transition Temperature of a Polymer (Polyamide) Blend Using MDSC Identification of Different Crystalline Forms of Sorbitol by DSC Two Phase Polymer System Studied by Temperature Dependent Pulsed Force Microscopy and Force versus Distance Curves Characterization of an Epoxy Resin Compound by MDSC Characterization of EPDM Rubber by TGA and Hi-Res TGA Characterization of the Glass Transition Temperature of Petroleum Pitch by MDSC Nylon 6.6 Characterization by MDSC® Characterization of a Polyurethane Hot Melt Adhesive by DSC and DMA Characterization of a PTFE/PEEK/Carbon Fiber Blend by TGA and Hi-Res™ TGA PTFE/PEEK/Carbon Fiber Blend Analysis by DSC Characterization of a Polyester Resin/Catalyst System by TGA. 6 TA 001k .□ □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ TN052 TN051 TN050 TN049 TN048 TN047 TN046 TN045 TN044 TN041 TN040 TN039 TN035 TN034 TN031 TN030 TN027 TN026 TN025 TN024 TN021 TN020 □ □ □ □ □ □ TN018 TN017 TN015 TN014 TN011 TN010 □ □ □ □ □ TN008 TN007 TN005 TN002 TN001 Cleaning of DSC Pans Installation Requirements for Thermal Analysis/Rheology Systems Testing Laboratories for Thermal Analysis (formerly TA034) Common PID Settings Polymer Heats of Fusion Using the Heater PID Method Segment ISO Thermal Methods Choosing Conditions in Modulated DSC® Purge Gas Recommendations for Use in Modulated DSC® Choosing Proper Tubing for Purge Gas Connections Optimizing Stepwise Isothermal Experiments in Hi-Res TGA Thermal Analysis Reference Books Installation Instructions Modulated DSC: A Simple Technique with Significant Benefits Calibration of TMA According to ASTM Standard Method E831 Determining Minimum Usable Sample Thickness in TMA Guidelines for Performing DMA Creep Experiments Common Metric Conversions Utilizing the Event Switch TGA Temperature Calibration Using Cure Temperature Standards ASTM Thermal Methods Automated Analysis of Specific Heat/Cool Segments in DSC Cyclic Experiments Guide for Choosing DSC Pans Experimental Considerations for Thermal Conductivity by MDSC® Literature Values for Water Specific Heat Capacity Simulating DTUL (ASTM D648) Experiments with the TMA Enthalpy of Melting for Standards Standard Terminology for Abbreviated Terms Relating to Plastics. □ TS068 □ TS067 □ □ □ □ □ □ TS066 TS065 TS064 TS063 TS062 TS061 □ TS060 □ □ □ TS054 TS053 TS052 □ □ □ TS050 TS049 TS048 □ TS047 □ □ TS046 TS045 □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ □ TS044 TS043 TS042 TS041 TS040 TS039 TS038 TS037 TS036 TS034 TS033 TS032 TS031 TS030 TS029 TS028 TS027 TS026 TS025 TS024 TS023 TS022 TS021 TS020 TS019 TS018 TS017 TS016 TS015 DSC and DMA Determination of Crystallinity of a Common Automotive Thermoplastic Characterization of an Acrylic/Melamine Copolymer Blend by DSC and DMA Characterization of Epoxy Reinforced Glass by DSC and DMA Characterization of EPDM Rubber by DSC and DMA Measurement of the Glass Transition Temperature Using DMA Determining the Optimum Sample Size for Testing of Films by DMA Effect of Frequency on the Modulus and Glass Transition Temperature of PET Determination of the Linear Viscoelastic Region of a Polymer Using Strain Sweep by DMA Characterization of Protein Denaturation by DSC Using High Volume Sample Pans Characterization of the Degree of Cure of Thermosetting Resins by DSC Polymer Melt Characterization and Reproducibility by Micro Thermal Analysis Multi-Layered Polymer Film Characterized by Micro Thermal Analysis .Local Thermal Analysis Characterization of a Styrene Pigment/Resin Sample by MDSC Characterization of Packaging Film Performance by DMA Creep Recovery Characterization of Packaging Film Performance by DMA Storage Modulus Analysis Characterization of Packaging Film Performance by DMA Creep Compliance Analysis Characterization of Printed Circuit Board materials by DMA Characterization of the Effect of Water as a Plasticizer on Lactose by MDSC® Characterization of Semi-Crystalline Pharmaceutical Compounds by MDSC® Characterization of the Glass Transition Temperature of Lactose by MDSC® Subambient Characterization of Soft Foam Material by DMA Characterization of Polyvinyl Chloride (PVC) by MDSC® Characterization of Polyvinyl Chloride (PVC) by DMA Characterization of Polyurethane by TGA and Hi-Res TGA Characterization of Polyurethane by MDSC® Determination of Curie Point Temperature by TGA Characterization of Polymer Film by TMA Penetration Characterization of Epoxy Prepregs by DSC Determination of Oil in Rubber by Vacuum TGA Analysis of Photocured Adhesives by DPC Stress/Strain Evaluation of Fibers Using TMA Determination of Fiber Saturation Point in Whole Wood Using DSC TGA Characterization of Gypsum in Stucco Investigation of the Curie Point by MDSC® Oxidative Stability of Polyolefins Determination of Calcium Sulfate Hydrate in Cement by DSC Measurement of Aging Effects on Amorphous PET Quantifying Polyethylene Terephthalate/ Polycarbonate Blends Evaluation of Inorganic Phase Transitions Determination of Polymer Blend Compositions Detecting Crystallinity Differences in Engineering Thermoplastics Determination of Initial Crystallinity by Modulated DSC® Measuring and Controlling Residual Solvent Levels in Wire Coatings Measurement of the Degree of Cure in Discrete Wired Circuit Boards Separation of Free and Bound Water in Pharmaceuticals Comparison of Elastomeric Shock Mounts (Vibration Dampers) Characterization of Resin Curing Using DMA/DEA/Controlled Stress Rheology 7 TA 001k . com To contact your local TA Instruments representative visit our website at www. 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[email protected] United Kingdom • Phone: 44-1-293-658900 • Fax: 44-1-293-658901 • E-mail: uk@tainstruments.□ □ □ □ □ □ □ □ TS014 TS013 TS012 TS011 TS010 TS009 TS008 TS007 □ TS005 □ □ □ □ □ TS004 TS003 TS002 TS001 RS040 Analysis of Polymer Decompositions by TGA-Mass Spectrometry Clarification of Inorganic Decomposition by TGA-Mass Spectrometry Evaluation of Cracking in Polymers Determination of Composite Cure Pigmentation Effects on Polyethylene Crystallization Predicting Printed Circuit Board Delamination Long Term Stability Testing of Printing Inks by DSC Thermal Stability Determination of Bonded Silicas for Use in Packing Columns by TGA Determination of the Relative Oxidative Stability of Polyethylene Bottle Tops by DSC Rapid Determination of Carbon Black in Elastomers Thermal History Determination of Textured Polyester Yarns Determination of the Dimensional Stability of a Thin PET Film Storage Effects of Tg for Epoxy Molding Compound Characterization of Heat Shrink Films Using DMA Film/Fiber Clamps and Controlled Force Mode Copyright 2005 TA Instruments TA Instruments United States.com Spain • Phone: 34-93-600-9300 • Fax: 34-93-325-9896 • E-mail:
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